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Diesel Analysis and Specifications

Flash Point

ASTM D-56: Standard Test Method for Flash Point by Tag Closed Tester

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Flash point determines the maximum temperature at which the fuel can be stored and handled without serious fire hazard

#1 Diesel, minimum 100.4° F

#2 Diesel, minimum 125.6° F

There is a flash point waiver to 100.4° F if a cloud point of -12° C (10.4° F) or below is specified during the coldest months. (November through March)

      Flash Point Testing

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Distillation

ASTM D-86: Standard Test Method for Distillation of Petroleum Products at Atmospheric Pressure

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Test Method D 86 for distillation provides another measure of the volatility of fuels.  The distillation characteristics affect starting, drivability, dilution of the engine oil, fuel economy and carburetor icing.  The temperatures are recorded at which 10%, 50% and 90% evaporation occur.  These temperatures are used to characterize whether the distillation meets the ASTM specifications. 

Specification for the temperature when 90% of the distillation is complete – (T90).

#1 Diesel maximum 550.4° F

#2 Diesel minimum 539.6° F

#2 Diesel maximum 640.4° F

Manual Distillation Units

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Sulfur

ASTM D-2622:  Standard Test Method for Sulfur in Petroleum Products by Wavelength Dispersive X-ray Fluorescence Spectrometry

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Sulfur affects the amount of particulate emissions emitted into the environment, cylinder wear, and deposits in internal combustion engines.

#1 Low Sulfur Diesel, maximum 0.05% mass (500 ppm)

#1 Ultra Low Sulfur Diesel, maximum 0.0015% mass (15 ppm)

#2 Low Sulfur Diesel, maximum 0.05% mass (500 ppm)

#2 Ultra Low Sulfur Diesel, maximum 0.0015% mass (15 ppm)

#1 or #2 Non Road Diesel (dyed, tax exempt), maximum  0.50% mass (5,000 ppm)

Sulfur Analysis using X-ray Fluorescence

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Cloud Point

ASTM D2500: Standard Test Method for Cloud Point of Petroleum Products

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The cloud point of a fuel is a guide to the temperature at which it may clog filter systems and restrict flow.  At very low temperatures wax crystals may precipitate out of the diesel fuel, blocking the fuel system lines and filters causing malfunctioning or stalling of the engine.  In Colorado, the requirements for cloud point start in October and continue through March, with the temperature requirements becoming colder through January and gradually warming up into March.  Colorado is also divided geographically into East and West along the 1050 longitude.  The requirements for Eastern Colorado are less restrictive than for Western Colorado, due to differences in mean elevation and temperature.  

  East 105° longitude West 105° longitude
October -2° C   (28.4° F) -8° C  (17.6° F)
November -12° C  (10.4° F) -18° C  (-0.4° F)
December -14° C  (6.8° F) -25° C  (-13° F)
January -19° C  (-2.2° F) -30° C  (-22° F)
February -15° C  (5° F) -24° C  (-11.2° F)
March -12° C  (10.4° F) -16° C  (3.2° F)

Cloud Point Analysis and two cloud point vials showing cloud point on the right.

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Calculated Cetane Index

ASTM D-4737:  Standard Test Method for Calculated Cetane Index by Four Variable Equation.

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The Cetane Number measures the ignition quality of diesel fuel based on ignition delay in an engine. The higher the cetane number, the shorter the ignition delay and the better the ignition quality of the fuel.

#1 Diesel (low sulfur) minimum 40

#2 Diesel (low sulfur) minimum 40

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